Broad Spectrum SPF 19.9, PFA (PPD) 14.3 Sunscreen Cream Formula Ref: CAB6-158 (Batch JZ2-122)

Hallstar

Phase

Product

INCI Name

Supplier

Volume

Dow Corning® 345 Fluid

Cyclopentasiloxane, Cyclohexasiloxane

4.00

Velvesil™ 125

Cyclopentasiloxane, C30-45 Alkyl Cetearyl Dimethicone Crosspolymer

4.50

Water [Deionized]

50.05

Versene™ NA,

Disodium EDTA

0.10

Superol™ K, Glycerine 99.7% USP/FCC Kosher

Glycerin

4.00

Mikrokill® COS

Phenoxyethanol, Caprylyl Glycol, Chlorphenesin

1.00

X-Tend™ 226

Phenethyl Benzoate

5.00

HallBrite® HS USP

Homosalate [Homosalate]

7.50

HallBrite® OS USP

Ethylhexyl Salicylate [Octisalate]

5.00

Neo Heliopan® 303

Octocrylene [Octocrylene]

2.75

SolaStay® S1,

Ethylhexyl Methoxycrylene

3.25

Parsol® 1789

Butyl Methoxydibenzoylmethane [Avobenzone]

3.00

HallStar® GMS SE/AS

Glyceryl Stearate, PEG-100 Stearate

1.00

HallStar® TA-1618 Cetearyl Alcoho

Cetearyl Alcohol

0.35

Ganex® V-220

VP/Eicosene Copolymer

1.00

Emulsiphos®,

Potassium Cetyl Phosphate, Hydrogenated Palm Glycerides

3.00

Simulgel™ 600

Acrylamide/Sodium Acryloyldimethyltaurate Copolymer, Isohexadecane, Polysorbate 80

2.50

MSS-500W

Silica

2.00

Preparation:

In a suitably rated vessel, premix 1 and 2 until homogeneous and smooth, then set aside for later use. Meanwhile add 3 and 4 to main vessel, commence center-stir (prop) mixing, start heating to 85°C, and add preblended 5 and 6. To a secondary vessel add 7 – 11, start mixing, add 12 and, when dissolved, heat to 85°C, then add 13 – 16 in order. With both phases at 85°C and homogeneous, add oil phase (7 – 16) to water phase (3 – 6) with stirring and stop heating. After mixing for ten minutes, homogenize until batch reaches 55°C, and then resume sweep mixing while cooling. At 50°C or lower, add 17 and when smooth add premix of 1 and 2. When again smooth, add 18, replace any water lost to evaporation, and mix until smooth. When at desired filling temperature, stop cooling and mixing, perform final quality assurance checks and package product.

Notes:

PRODUCT PROPERTIES (25°C) Appearance: light yellow cream Viscosity (RV, T-D, 5, 20 & 100 rpm, cP): 75600, 22500, 6420 pH: 6.4

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