Broad Spectrum SPF 54, PFA (PPD) 27 Sunscreen Cream

Hallstar
Phase
Product
INCI Name
Supplier
Volume
A
Finsolv® TN
C12-15 Alkyl Benzoate
Innospec
5.00
Neo Heliopan® 303
Octocrylene [Octocrylene]
Symrise
10.00
SolaStay® S1
Ethylhexyl Methoxycrylene
HallStar
3.40
B
TTO-80A
Titanium Dioxide [Titanium Dioxide], Aluminum Hydroxide
Kobo Products
4.10
C
HallStar® GMS
Glyceryl Stearate
HallStar
1.50
HallStar® GMS SE/AS
Glyceryl Stearate, PEG-100 Stearate
HallStar
2.00
HallStar® CO-1895 Stearyl Alcohol NF
Stearyl Alcohol
HallStar
0.50
Emulsiphos®
Potassium Cetyl Phosphate, Hydrogenated Palm Glycerides
Symrise
2.00
D
Neo Heliopan® 357
Butyl Methoxydibenzoylmethane [Avobenzone]
Symrise
3.00
E
-
Water [Deionized]
59.91
F
Versene™ NA
Disodium EDTA
Dow Chemical
0.05
G
Pemulen® TR-2 Polymer
Acrylates/C10-30 Alkyl Acrylate Crosspolymer
Noveon
0.30
H
CoSept™ PEP
Phenoxyethanol, Methylparaben, Ethylparaben, Butylparaben, Propylparaben, Isobutylparaben
HallStar
0.50
Superol™ K Glycerine 99.7% USP/FCC Kosher
Glycerin
P&G Chemicals
4.00
I
Potassium Hydroxide Flake [10% aqueous]
Potassium Hydroxide
J.T. Baker
1.74
J
MSS-500W
Silica
Kobo Products
2.00

Preparation:

In secondary vessel, combine A and start mixing. Slowly add B with continued mixing. Heat this oil phase to 80°C, then, in order, add C. When A–C is homogeneous, add D and mix until totally dissolved. To the main vessel, add E and start mixing. Add F and when dissolved, add G. When fully incorporated, start heating to 80°C and add premix of H. When oil and water phases are uniform and at the defined temperatures, add the oil phase (A–D) to the water phase (E–H) with strong mixing and without aeration. Start homogenizing intensively and start cooling. When the batch is at 45°C, add I and keep homogenizing intensively. Stop homogenizing and resume sweep mixing. Add J and mix well. When the batch is uniform, add deionized water to correct for evaporative losses. Continue mixing until a smooth, homogeneous cream results. Perform final quality assurance checks.

Notes:

PRODUCT PROPERTIES (25°C) Appearance: Cream-colored soft cream Viscosity (RV, T-D, 5, 20 & 100 rpm, cP): 92000, 27400 & 7200 pH: 6.6 Stability: acceptable through three freeze thaw cycles and after 1.5 months at 45°C
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